State whether the following statements regarding fractional distillation are True or False:
$(i)$ The freezing of vapour of a liquid with a high boiling point takes place first.
$(ii)$ In the column,the more volatile liquid is present in a higher concentration in the vapour phase at higher levels.
$(iii)$ The condensed liquid flows down and provides heat to the vaporizing liquid.
$(iv)$ The liquid with the highest boiling point reaches the top of the column.

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(N/A) $(i)$ False,$(ii)$ True,$(iii)$ True,$(iv)$ False.

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Which of the following can be purified by sublimation?

Using the given figure,the ratio of $R_f$ values of sample $A$ and sample $C$ is $x \times 10^{-2}$. The value of $x$ is . . . . . . . .
Table: Paper chromatography of Samples
| Component | Distance from base line (cm) |
| :--- | :--- |
| Sample $A$ | $5.0$ |
| Sample $B$ | $6.5$ |
| Sample $C$ | $10.0$ |
| Solvent front | $12.5$ |

How is glycerol separated from spent-lye in the soap industry?

Match items of Column-$I$ and Column-$II$.
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$A$. $H_2O / CH_2Cl_2$ $I$. Crystallization
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Correct match is:

Glycerol is purified by

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